Facility

The Laboratory is equipped with Zeiss/LEO Supra VP55 Scanning Electron Microscope (SEM) with a field emission electron gun (FEG), Energy Dispersive X-ray Spectroscope (EDS), SPI Sputter Coater (Sputter Module #11430, Carbon Coater Module #11428, Vacuum Control Base Module 110V #11425-AB) and the SEM sample preparation area.

Zeiss/LEO Supra VP55 Scanning Electron Microscope (SEM) with a field emission electron gun (FEG) and Energy Dispersive X-ray Spectroscope (EDS). 

Specification

   SEM

  • Resolution: 0.1nm at 15kV, 1.7nm at 1kV (HV), 2.0nm at 30kV (VP)
  • Accelerating voltage: 100V to 30kV
  • Six beam defining apertures
  • Secondary electron (SE) detector
  • Variable pressure secondary electron (VPSE) detector for VP mode
  • Scanning transmission electron microscopy (STEM) detector
  • 4 Quadrant solid state back scattered electron (BSE) detector
  • CCD camera with IP illumination
  • X-ray and external scan input panel
  • Microsoft Windows 2000 operating system and LEO32 software for total system control

   EDS

  • UltraDry Series EDS Detector with NORVAR light element window
  • NORAN System 7 Spectral Imaging System Ver.2 for image acquisition and analytical software package
  • COMPASS software for the automatic analysis of spectral imaging files collected with the NORAN System 7 Spectral Imaging System
  • Spectral Match software for least squares fitting and matching of spectra to spectral database
  • Digital imaging interface for electron microscope
  • Microscope Column Communication software
  • Microsoft Windows 7 operating system
SPI Sputter Coater modules

Specification

SPI Sputter Coater

  • Sputter Module #11430
  • Carbon Coater Module #11428
  • Vacuum Control Base Module 110V #11425-AB